Nanomaterials, with their unique properties and wide range of applications, have been at the forefront of scientific research and technological advancements. The synthesis and characterization of these materials play a crucial role in understanding their fundamental properties and optimizing their performance for various applications. Among the many aspects of nanomaterial research, nanoscale characterization methods are of paramount importance in deciphering the structural, chemical, and physical properties of these materials at the atomic and molecular level.